(Hexane-1,6-diamine)–silicalite-1 is crystallised at 100 °C from the reaction mixture 10M2O/60SiO2/10H2N[CH2]6NH2/3000H2O (M = K or Rb); quaternary ammonium ions are not essential for the crystallisation of the silicalite-1 framework.
A. Araya and B. M. Lowe, J. Chem. Soc., Chem. Commun., 1987, 1455 DOI: 10.1039/C39870001455
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