The thermal, [1,3]-shift siloxy-Cope, ring expansion in shown to be highly favoured relative to the [3,3]-shift for the large-ring system required for the synthesis of muscone.
R. W. Thies and K. P. Daruwala, J. Chem. Soc., Chem. Commun., 1985, 1188 DOI: 10.1039/C39850001188
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