Asymmetric incorporation of 18O into pyrophosphate to perturb the 31P n.m.r. resonance frequency allows determination of the 31P–31P germinal coupling constant in this otherwise symmetrical molecule.
T. M. Marschner, M. A. Reynolds, N. J. Oppenheimer and G. L. Kenyon, J. Chem. Soc., Chem. Commun., 1983, 1289 DOI: 10.1039/C39830001289
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