Dibutyl and monobutyl phosphates were determined by gas chromatography. A procedure involving separation, extraction and methylation was developed and it was found that the use of a flame-photometric detector gave better results. The detection limits of 5 × 10–8 g were found for both dibutyl and monobutyl phosphates.
C. Kuo, J. Shih and Y. Yeh, Analyst, 1982, 107, 1190 DOI: 10.1039/AN9820701190
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