Dehydrogenation to the corresponding diketone occurs to the extent of 16% and 42% respectively in the flash vacuum pyrolysis of 3,6-dimethyl-1,2-dioxacyclo-hexane and 2,3-dioxabicyclo[2.2.2]octane, but is unimportant in similar pyrolyses of 3,5-dimethyl-1,2-dioxacyclopentane and 2,3-dioxabicyclo [2.2.1] heptane.
A. J. Bloodworth and D. S. Baker, J. Chem. Soc., Chem. Commun., 1981, 547 DOI: 10.1039/C39810000547
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