The benzyne ligand in Os3(CO)9(PEt)(C6H4) is shown by X-ray crystallography to be asymmetrically bound with one carbon atom σ-bonded to one osmium while a second bridges the two other metal atoms; a low energy process interchanges these two sites in solution.
S. C. Brown, J. Evans and L. E. Smart, J. Chem. Soc., Chem. Commun., 1980, 1021 DOI: 10.1039/C39800001021
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