A vinylogous, base-catalysed acyloin rearrangement leading to products (4) and (5) possessing the twistane (tricyclo[4.4.0.03,8]decane) ring skeleton is reported; an X-ray crystal structure analysis of (5) was performed.
T. J. Greenhough, J. R. Scheffer, J. Trotter and Y. Wong, J. Chem. Soc., Chem. Commun., 1979, 933 DOI: 10.1039/C39790000933
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