A general method for the synthesis of a new type of compounds, unesterified acylphosphonic acids, is described, involving reactions of tris(trimethylsilyl) phosphite with acyl chlorides followed by solvolysis of the products using aniline-containing alcohols.
M. Sekine and T. Hata, J. Chem. Soc., Chem. Commun., 1978, 285b DOI: 10.1039/C3978000285B
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