The reaction of Re, KReO4, or ReS2 with an excess of Na2CO3 or K2CO3 and S at 750 °C yields MI4Re6S12, ReIII compounds containing Re6 octahedra located in cubes of sulphide ions with sulphide and disulphide bridges between octahedra.
S. Chen and W. R. Robinson, J. Chem. Soc., Chem. Commun., 1978, 879 DOI: 10.1039/C39780000879
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