SCHEDULED MAINTENANCE:
Syntheses of 6-endo-(VI) and 6-exo-acetoxy-4-methylene-2-oxabicyclo[3.3.0]oct-7-en-3-one (XI) from readily available bromolactones (I) and (VII) have been accomplished through formation and dehydrohalogenation of intermediate iodoacetates.
S. M. Ali and S. M. Roberts, J. Chem. Soc., Chem. Commun., 1976, 584 DOI: 10.1039/C39760000584
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