The n.m.r. spectra of a series of halogeno-sulphinamides are described at varying temperatures and concentrations; the spectra are intepreted in terms of restricted torsion around the N–S bond (ΔG‡ 35–60 kJ mol–1) and rapid halogen-exchange reactions in the case of the chloro- and bromo-compounds.
W. R. Jackson, T. G. Kee and W. B. Jennings, J. Chem. Soc., Chem. Commun., 1972, 1154 DOI: 10.1039/C39720001154
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