An unusual cycloaddition reaction of [2,2](2,5)furanophane with tetrachlorocyclopropene yields a crystalline 1:1 adduct, the structure of which has been determined by X-ray diffraction to be 5,6,7,7-tetrachloro-16,17-syn-dioxahexacyclo[9,2,2,1,1,4,8, 04,14, 08,15]-heptadeca-5,12-diene.
M. A. Battiste, L. A. Kapicak, M. Mathew and G. J. Palenik, J. Chem. Soc. D, 1971, 1536 DOI: 10.1039/C29710001536
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