Oxidation of cyclo-oct-5-ene-trans-1,2-diol with dimethyl sulphoxide and acetic anhydride gives cyclo-oct-5-ene-1,2-dione, which with ethylene glycol and toluene-p-sulphonic acid forms a monoacetal and two diacetals, whose structures have been assigned on the basis of deacetalization experiments and mass and 1H n.m.r. spectroscopy.
P. Yates and E. G. Lewars, J. Chem. Soc. D, 1971, 1537 DOI: 10.1039/C29710001537
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