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Issue 11, 2019
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Mechanochemical synthesis of N-doped porous carbon at room temperature

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Abstract

We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m2 g−1.

Graphical abstract: Mechanochemical synthesis of N-doped porous carbon at room temperature

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Publication details

The article was received on 31 Jan 2019, accepted on 25 Feb 2019 and first published on 25 Feb 2019


Article type: Communication
DOI: 10.1039/C9NR01019J
Nanoscale, 2019,11, 4712-4718
  • Open access: Creative Commons BY-NC license
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    Mechanochemical synthesis of N-doped porous carbon at room temperature

    M. E. Casco, S. Kirchhoff, D. Leistenschneider, M. Rauche, E. Brunner and L. Borchardt, Nanoscale, 2019, 11, 4712
    DOI: 10.1039/C9NR01019J

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