Issue 11, 2019

Mechanochemical synthesis of N-doped porous carbon at room temperature

Abstract

We report the one-pot mechanochemical synthesis of N-doped porous carbons at room temperature using a planetary ball mill. The fast reaction (5 minutes) between calcium carbide and cyanuric chloride proceeds in absence of any solvent and displays a facile bottom-up strategy that completely avoids typical thermal carbonization steps and directly yields a N-doped porous carbon containing 16 wt% of nitrogen and exhibiting a surface area of 1080 m2 g−1.

Graphical abstract: Mechanochemical synthesis of N-doped porous carbon at room temperature

Supplementary files

Article information

Article type
Communication
Submitted
31 Jan 2019
Accepted
25 Feb 2019
First published
25 Feb 2019
This article is Open Access
Creative Commons BY-NC license

Nanoscale, 2019,11, 4712-4718

Mechanochemical synthesis of N-doped porous carbon at room temperature

M. E. Casco, S. Kirchhoff, D. Leistenschneider, M. Rauche, E. Brunner and L. Borchardt, Nanoscale, 2019, 11, 4712 DOI: 10.1039/C9NR01019J

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