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Issue 3, 2017
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Continuous flow dynamic kinetic resolution of rac-1-phenylethanol using a single packed-bed containing immobilized CAL-B lipase and VOSO4 as racemization catalysts

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Abstract

Herein, we report a method for the continuous flow DKR of rac-1-phenylethanol catalyzed by CAL-B and VOSO4, using a single packed-bed containing both catalysts. Taking advantage of continuous flow techniques to circumvent compatibility issues, the DKR of rac-1-phenylethanol could be performed continuously to give enantiopure (R)-esters with excellent conversions and high productivities.

Graphical abstract: Continuous flow dynamic kinetic resolution of rac-1-phenylethanol using a single packed-bed containing immobilized CAL-B lipase and VOSO4 as racemization catalysts

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Article information


Submitted
04 Jan 2017
Accepted
15 Feb 2017
First published
15 Feb 2017

React. Chem. Eng., 2017,2, 375-381
Article type
Paper

Continuous flow dynamic kinetic resolution of rac-1-phenylethanol using a single packed-bed containing immobilized CAL-B lipase and VOSO4 as racemization catalysts

A. S. de Miranda, M. V. de M. Silva, F. C. Dias, S. P. de Souza, R. A. C. Leão and R. O. M. A. de Souza, React. Chem. Eng., 2017, 2, 375
DOI: 10.1039/C7RE00003K

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