The first synthesis of planar-chiral benzosiloloferrocenes was achieved by the intramolecular reaction of 2-(dimethylhydrosilyl)arylferrocenes. The enantioselective cross dehydrogenative coupling of an sp2 C–H bond of ferrocene with a Si–H bond proceeded efficiently with the use of a Rh-chiral diene catalyst.
T. Shibata, T. Shizuno and T. Sasaki, Chem. Commun., 2015, 51, 7802 DOI: 10.1039/C5CC00723B
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