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The reaction of a series of organolanthanide fragments of samarium and thulium with phenanthroline is reported. All adducts couple in the 4-position of the phenanthroline ligand to yield the 4–4′ dimers when they crystallize. The analysis of the solution structure revealed a thermally reversible C–C coupling in all cases.
G. Nocton and L. Ricard, Chem. Commun., 2015, 51, 3578 DOI: 10.1039/C5CC00289C
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