Issue 4, 2010
From the journal:

CrystEngComm

Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazinemacrocycle†

Conor Dawson,a   Peter N. Horton,b   Michael B. Hursthouseb  and  Stuart L. James*a  

* Corresponding authors

a Centre for the Theory and Application of Catalysis, School of Chemistry and Chemical Engineering, Queen's University Belfast, David Keir Building, Stranmillis Road, Belfast, Northern Ireland, UK
E-mail: s.james@qub.ac.uk

b Department of Chemistry, University of Southampton, Highfield, Southampton, UK

Abstract

The 4 + 4 macrocycle {CH2C6H4CH2N(CH2CH2)2N}4 with alternating para-phenylene and piperazine groups linked by methylene spacers adopts tubular stacking in the crystal with 36% solvent-filled volume.

Graphical abstract: Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle

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Article information

DOI
https://doi.org/10.1039/B917953D
Article type
Communication
Submitted
01 Sep 2009
Accepted
30 Oct 2009
First published
10 Nov 2009

CrystEngComm, 2010,12, 1048-1050

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Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle

C. Dawson, P. N. Horton, M. B. Hursthouse and S. L. James, CrystEngComm, 2010, 12, 1048 DOI: 10.1039/B917953D

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