Increasing the time allowed for hydrothermal crystallisation during high temperature (150 °C) synthesis of MCM-41 appears to result in some ordering (nanocrystallites) within the pore walls which is accompanied by increase in pore wall thickness, pore size, silica condensation and the formation of elongated or rod-like particles.
Observation of some pore wall ordering in mesoporous silica
R. Mokaya, Chem. Commun., 2001, 1092 DOI: 10.1039/B101812O
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