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Issue 14, 2000
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Solvent directing immediate fluorination of aromatic ketones using 1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate)The results of characterisation of 2a, 2b, 3a, 3b, 4a, 4b, 5a, 6a and 9 are available as electronic supplementary information (ESI). See http://www.rsc.org/suppdata/cc/b0/b003488f/

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Abstract

Reactions of aryl alkyl ketones with 1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate) (AccufluorTM NFTh) in methanol result in selective and almost quantitative formation of the corresponding α-fluoroketones, while in acetonitrile exclusive fluorofunctionalisation of the activated aromatic ring take place.

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Article information


Submitted
02 May 2000
Accepted
12 Jun 2000
First published
29 Jun 2000

Chem. Commun., 2000, 1323-1324
Article type
Communication

Solvent directing immediate fluorination of aromatic ketones using 1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2.2.2]octane bis(tetrafluoroborate)

S. Stavber, M. Jereb and M. Zupan, Chem. Commun., 2000, 1323
DOI: 10.1039/B003488F

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