High-resolution 1H MAS NMR spectra of 2∶1 phyllosilicates

María D. Alba; Ana I. Becerro; Miguel A. Castro; Ana C. Perdigón

doi:10.1039/A906577F

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High-resolution ¹H MAS NMRspectra of 2∶1 phyllosilicates

María D. Alba,*^a Ana I. Becerro,^a Miguel A. Castro^a and Ana C. Perdigón^a

Author affiliations

* Corresponding authors

^a Departamento de Química Inorgánica, Instituto de Ciencia de Materiales, Universidad de Sevilla, Consejo Superior de Investigaciones Científicas, Avda. Américo Vespucio s/n., Sevilla, Spain.
E-mail: alba@cica.es

Abstract

Solid-state ¹H MAS NMR at high magnetic fields and high spinning speeds provides a powerful means of identifying the different proton sites in smectites and affects information on the octahedral nature, the octahedral layer charge deficit and the charges on the cations residing in the interlayer space of the silicate.

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Article information

DOI: https://doi.org/10.1039/A906577F
Article type: Communication
Submitted: 09 Aug 1999
Accepted: 22 Nov 1999
First published: 24 Dec 1999

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Chem. Commun., 2000, 37-38

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High-resolution ¹H MAS NMR spectra of 2∶1 phyllosilicates

M. D. Alba, A. I. Becerro, M. A. Castro and A. C. Perdigón, Chem. Commun., 2000, 37 DOI: 10.1039/A906577F

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