Excess octaphenylcyclotetrasiloxane [{SiPh2(µ-O)}4] and C60 in toluene affords the 1:1 supramolecular complex as a hemi-toluene solvate where the fullerenes are arranged in double columnar arrays shrouded by edge on, interlocking siloxanes.
I. E. Grey, Chem. Commun., 1999, 1139 DOI: 10.1039/A901719D
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