Hydrolysis of {Li[BunC(NBut)2]}2, prepared from LiBun and ButNCNBut in hexanes, produced the nineteen atom cluster {Li[BunC(NBut)2]}4·Li2O; an X-ray structure determination revealed an Li2O molecule encapsulated by two eight-membered Li2N4C2 rings.
T. Chivers, A. Downard and G. P. A. Yap, J. Chem. Soc., Dalton Trans., 1998, 2603 DOI: 10.1039/A804955F
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