Treatment of (1-hydroperoxy)cyclohexyloxyethyl acrylate with either iron(II) sulfate or iron(II) sulfate/copper(II) chloride affords novel 13-membered macrolides via tandem radical scission-cyclisation reactions.
K. J. McCullough, Y. Motomura, A. Masuyama and M. Nojima, Chem. Commun., 1998, 1173 DOI: 10.1039/A801802B
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