Issue 7, 1998

Non-planar structures of Et3N and Pri3N: a contradiction between the X-ray, and NMR and electron diffraction data for Pri3N

Abstract

The crystal structures of Et3N and Pri3N were determined by X-ray analysis using the in situ crystallization technique for single crystal growth on the diffractometer; both have a pyramidal configuration of the nitrogen atom, even Pri3N, which was considered to be planar in accord with electron diffraction and NMR data.

Article information

Article type
Paper

Chem. Commun., 1998, 781-782

Non-planar structures of Et3N and Pri3N: a contradiction between the X-ray, and NMR and electron diffraction data for Pri3N

R. Boese, D. Bläser, M. Y. Antipin, R. Boese, M. Y. Antipin, V. Chaplinski and A. de Meijere, Chem. Commun., 1998, 781 DOI: 10.1039/A708399H

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