The major products of the interaction between triethyl phosphite and 3-fluoropropanoyl chloride at room temperature are diethyl (E)-1-(3-fluoropropanoyloxy)-3-fluoroprop-1-enylphosphonate 3 and diethyl 1-(diethoxyphosphoryl)-3-fluoropropyl phosphate 4, which result from concurrent 1:2 and 2:1 rections, respectively.
H. R. Hudson, M. Pianka and W. Jun, Chem. Commun., 1996, 2445 DOI: 10.1039/CC9960002445
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