A tetramethylethylene bridged ferrocene 1 and cobaltocene 3 are synthesised in two steps from 2-tert-butyl-6,6-dimethylfluvene. Both can be oxidised to the corresponding cations, 2 and 4, the single-crystal X-ray structures of which have been determined.
M. J. Drewitt, S. Barlow, D. O'Hare, J. M. Nelson, P. Nguyen and I. Manners, Chem. Commun., 1996, 2153 DOI: 10.1039/CC9960002153
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