Treatment of [VCl3(thf)3](thf = tetrahydrofuran) with Li[C6H2(CF3)3-2,4,6] affords the first early transition-metal complexes containing the σ-bonded fluoromes ligand; the molecular structures of [V{C6H2(CF3)3-2,4,6}2Cl(thf)] 1 and [V{C6H2(CF3)3-2,4,6}3OLi(thf)3] 2 are described.
V. C. Gibson, C. Redshaw, L. J. Sequeira, K. B. Dillon, W. Clegg and M. R. J. Elsegood, Chem. Commun., 1996, 2151 DOI: 10.1039/CC9960002151
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