The cerium-mediated reaction between lithio (diethyldifluoromethyl)-phosphonate 2 proceeds smoothly to afford good yields of ketophosphonates; the reaction with DMF led to the formation of the corresponding aldehyde which was isolated as a hydrate with interesting and useful properties.
T. P. Lequeux and J. M. Percy, J. Chem. Soc., Chem. Commun., 1995, 2111 DOI: 10.1039/C39950002111
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