A new method for evaluating the efficiency of nickel macrocyclic electrocatalysts for reduction of CO2 to CO using a rotating copper disc electrode has led to the discovery of a new highly active complex, [NiL2]2+[L2= 3,10-dimethyl-1,3,5,8,10,12-hexaazacyclotetradecane (diazacyclam)].
C. I. Smith, J. A. Crayston and R. W. Hay, J. Chem. Soc., Dalton Trans., 1993, 3267 DOI: 10.1039/DT9930003267
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