Complete exchange of protons with deuterons in conventional FAB-MS can be achieved by introducing samples into the mass spectrometer via microbore-HPLC using a deuteriated mobile phase; structural information of analytes in a mixture can be obtained by using this system.
T. McLean, A. P. New, N. J. Haskins and P. Camilleri, J. Chem. Soc., Chem. Commun., 1992, 1773 DOI: 10.1039/C39920001773
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