Topotactic electrochemical reduction of metallic KCu4S3 in Cu+ electrolytes results in the formation of semiconducting KCu5S3via anion p-band hole annihilation in a reversible process.
F. Viola and R. Schöllhorn, J. Chem. Soc., Chem. Commun., 1992, 907 DOI: 10.1039/C39920000907
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