The sterocontrolled synthesis of trans-octahydroanthracenes 3, 11 and 14 through implementation of an efficient and highly regioselective 6-endo-trig-aryl radical cyclisation of the respective 2-(o-bromobenzyl)-1-methylenecyclohexanes 2, 10 and 13, with tri-n-butyltin hydride is reported, along with a single crystal X-ray structure determination of 11.
S. Pal, M. Mukherjee, D. Podder, A. K. Mukherjee and U. R. Ghatak, J. Chem. Soc., Chem. Commun., 1991, 1591 DOI: 10.1039/C39910001591
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