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Issue 22, 1991
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A highly regioselective 6-endo-aryl radical cyclisation: stereocontrolled synthesis of trans-octahydroanthracenes

Abstract

The sterocontrolled synthesis of trans-octahydroanthracenes 3, 11 and 14 through implementation of an efficient and highly regioselective 6-endo-trig-aryl radical cyclisation of the respective 2-(o-bromobenzyl)-1-methylenecyclohexanes 2, 10 and 13, with tri-n-butyltin hydride is reported, along with a single crystal X-ray structure determination of 11.

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Article type: Paper
DOI: 10.1039/C39910001591
Citation: J. Chem. Soc., Chem. Commun., 1991,0, 1591-1593

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    A highly regioselective 6-endo-aryl radical cyclisation: stereocontrolled synthesis of trans-octahydroanthracenes

    S. Pal, M. Mukherjee, D. Podder, A. K. Mukherjee and U. R. Ghatak, J. Chem. Soc., Chem. Commun., 1991, 0, 1591
    DOI: 10.1039/C39910001591

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