A highly convergent and efficient synthesis of methylenomycin B has been achieved by the reaction of the lithium enolate of 4-chloro-4,5-dimethyl-5-hexen-3-one with phenylselenenyl bromide followed by selenoxide elimination.
J. Mathew, J. Chem. Soc., Chem. Commun., 1990, 1264 DOI: 10.1039/C39900001264
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