A quindecanuclear nickel–sulphur cluster compound with triphenylphosphine, Ni15(µ3-S)6(µ4-S)9(PPh3)6, is obtained from the reaction of NiCl2, PPh3, and Na2S in dimethylformamide–tetrahydrofuran and has been shown by X-ray single crystal structural analysis to be co-facial quater-octahedra in a chain.
M. Hong, Z. Huang and H. Liu, J. Chem. Soc., Chem. Commun., 1990, 1210 DOI: 10.1039/C39900001210
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