The reaction of [NH4]3[VS4] with 2,2′ : 6′,2″-terpyridine (terpy) in methanol gives the novel vanadium compound [V(S2)2(terpy)], the crystal structure of which has been determined by X-ray diffraction. Its formation is probably the simplest example of intramolecular coupling of sulphide ligands in a tetrathiometalate anion.
F. T. Al-Ani, D. L. Hughes and C. J. Pickett, J. Chem. Soc., Dalton Trans., 1988, 1705 DOI: 10.1039/DT9880001705
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