Bis(ethylenedithiolo)tetrathiafulvalene was prepared by a photochemical desulphurization of 4,5-ethylenedithiolo-1,3-dithiole-2-thione (1), and the effect of the type of solvent, nucleophilic agent and its concentration, and temperature on the yield of the reaction is discussed.
M. Šorm, S. Nešpůrek, O. Ryba and V. Kubánek, J. Chem. Soc., Chem. Commun., 1987, 696 DOI: 10.1039/C39870000696
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