Powder neutron diffraction has been used to measure directly the silicon–aluminium partitioning between the two tetrahedral sites in zeolite L; the similar environments of the two sites prevent simple measurement of this partitioning by 29Si n.m.r. spectroscopy, but enable its use as a probe of framework composition.
J. M. Newsam, J. Chem. Soc., Chem. Commun., 1987, 123 DOI: 10.1039/C39870000123
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