Electrolysis of alkylthioacetonitriles (1) in the presence of toluene-p-sulphonic acid as an electrolyte in methanol readily affords synthetically useful α-methoxylated sulphides (2) possibly by way of a Pummerer-type intermediate.
M. Kimura, K. Koie, S. Matsubara, Y. Sawaki and H. Iwamura, J. Chem. Soc., Chem. Commun., 1987, 122 DOI: 10.1039/C39870000122
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