SCHEDULED MAINTENANCE
The remarkably selective reaction of O,O,O-dialkyltrimethylsilylselenophosphates (1) in the presence of equimolar amounts of dialkyltrimethylsilyl phosphites (2) with sulphuryl chloride leading to tetra-alkyl symmetrical selenopyrophosphates (3) in excellent yields is reported.
R. Dembiński, R. Kamiński, J. Michalski and A. Skowrońska, J. Chem. Soc., Chem. Commun., 1986, 1770 DOI: 10.1039/C39860001770
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