The naturally occurring cyclopentenone, tetrahydrodicranenone B (1), has been synthesised from 6-methoxyindanone by a route which involves reductive alkylation and ozonolysis to the key cyclopentenone (3), followed by elongation of the lower side chain to give the alcohol (7), and functional group manipulation.
C. J. Moody, S. M. Roberts and J. Toczek, J. Chem. Soc., Chem. Commun., 1986, 1292 DOI: 10.1039/C39860001292
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