The radial electron distribution obtained from X-ray patterns has been used to study the structure of a poorly-crystalline vanadium–phosphorus mixed oxide (VPO) catalyst after selective oxidation of n-butane; the effective catalyst consists of a mixture of a crystallized (VO)2P2O7 phase (V4+) and an amorphous VPO phase (V5+) showing many corner-sharing VO6 octahedra.
G. Bergeret, J. P. Broyer, M. David, P. Gallezot, J. C. Volta and G. Hecquet, J. Chem. Soc., Chem. Commun., 1986, 825 DOI: 10.1039/C39860000825
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