Aqua ions of Mo3S44+ and Mo4S45+ have been obtained in high yield in a single electrochemical experiment, which is applicable also to the preparation of Mo3O44+ and Mo4O45+ and other analogous clusters.
P. Kathirgamanathan, M. Martinez and A. G. Sykes, J. Chem. Soc., Chem. Commun., 1985, 953 DOI: 10.1039/C39850000953
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