Sodium 2,6-diphenylbenzenethiolate react with [MoBr2(CO)4] to give the chelated η6-arene complex [Mo{(η6-Ph)PhC6H3S-2,6}(SC6H3Ph2-2,6)(CO)](1) in good yield, the X-ray crystal structure of which reveales a distored ‘piano-stool’ geometry.
P. T. Bishop, J. R. Dilworth and J. A. Zubieta, J. Chem. Soc., Chem. Commun., 1985, 257 DOI: 10.1039/C39850000257
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