Benzylic type di-Grignard reagents (2)–(5) and the mono-Grignard reagent (6) have been prepared by treating the appropriate organic chloride, for (2)–(6), or bromide, for (3) and (4), with magnesium anthracene in tetrahydroguran in yields of, repectively, 92–96%, and 60 and 84%.
C. L. Raston and G. Salem, J. Chem. Soc., Chem. Commun., 1984, 1702 DOI: 10.1039/C39840001702
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