The facile reaction of dicyclopentadienylhexacarbonyldichromium with stoicheiometric amounts of elemental sulphur in tetrahydrofuran or toluene at ambient temperature produces (η5-C5H5)2Cr2(CO)4S (1) and (η5-C5H5)2Cr2(CO)5S2(2) in isolated yields of 100 and 90%, respectively.
L. Y. Goh, T. W. Hambley and G. B. Robertson, J. Chem. Soc., Chem. Commun., 1983, 1458 DOI: 10.1039/C39830001458
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