SCHEDULED MAINTENANCE
Treatment of ω-substituted 1-alkynes (2) with 2 equiv. of trimethylstannylcopper–dimethyl sulphide (1) in tetrahydrofuran (–63 ° C)in the presence of 60 equiv. of methanol affords good to excellent yields of the corresponding 2-(trimethylstannyl)-1-alkenes (3).
E. Piers and J. M. Chong, J. Chem. Soc., Chem. Commun., 1983, 934 DOI: 10.1039/C39830000934
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