Readily available 3-(α-dialkylaminobenzylidene)-1-alkylthiotriazenes, when stirred in dichloromethane solution with copper(I) cyanide catalyst, give good yields of (E)-sulphenamidines (a new class of compounds): the mechanism of this extrusion reaction is discussed and the structure of one of the sulphenamidines has been established.
R. L. Beddoes, R. J. Cernik, O. S. Mills and F. Stansfield, J. Chem. Soc., Chem. Commun., 1983, 390 DOI: 10.1039/C39830000390
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