N.m.r. spectroscopy and X-ray crystallography show that oxidation of 5-substituted 4-acetyl-2-acetylamino-Δ2-1,3,4-thiadiazolines with m-chloroperbenzoic acid gives the corresponding Δ2-1,3,4-thiadiazoline 1-oxides; the novel reactions of the product (2a) are also described.
S. Kubota, K. Toyooka, N. Yamamoto, M. Shibuya and M. Kido, J. Chem. Soc., Chem. Commun., 1982, 901 DOI: 10.1039/C39820000901
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