New C-mercuriated sugars have been synthesised via hydroboration–transmetallation sequences; the bis(glycosyl)mercury compound (4) reacts very repidly with bromine chloride generated in situ from sodium bromide and chloramine-T, to give a high isolated yields of bromo-sugar (5)(87%).
L. D. Hall and J. Neeser, J. Chem. Soc., Chem. Commun., 1982, 887 DOI: 10.1039/C39820000887
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